Copper disulfide visualization in optic microscope

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jlribas jlribas
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Copper disulfide visualization in optic microscope

Dear all,
Someone knows any way of visualization deposition or aggregates forms of
copper disulfide or sulfide (CuS2 or CuS) by means of an optic
microscope. In its natural form this compund has no autofluorescence. It
colud be also any reaction that produce a color.

Thanks in advance
Best regards

--
Juan Luis Ribas
Servicio de Microscopía
Centro de Investigación, Tecnología e Innovación
Universidad de Sevilla
Av. Reina Mercedes 4b
41012 Sevilla

Tfno: 954559983
Barbara Foster Barbara Foster
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Re: Copper disulfide visualization in optic microscope

Dear Juan

My first reaction was for you to try polarized light microscopy.  I found an interesting article on-line from the American Minerologist, 1979 (King & Prewitt).  They indicate that the crystal structure they found was cubic, which would typically not respond to polarized light, CuS2 has anisotropic optical properties, which would indicate that it WOULD respond.  So my first response would still be for you to try Pol.  If you need a short class on how best to use this technique, I recommend that you contact my colleague, Phil Robinson (see email above).  For many years, he was a principal lecturer at the North Staffordshire Polytechnic and a senior instructor with the RMS, specializing in Pol.  He also knows everything there is to know about minerology and may have other suggestions for you.

Alternatively, if you are trying to produce a color, I would try dispersion staining from McCrone or, the lovely but old technique of Rheinberg illumination.  Both will "optically" stain your crystals.  If you are interested in learning more, contact me off line.

Good Hunting!

Barbara Foster, President and Sr. Consultant
Microscopy/Microscopy Education
7101 Royal Glen Trail, Suite A
McKinney TX 75070
P: (972)924-5310  Skype: fostermme
W: www.MicroscopyEducation.com

NEWS! Visit the NEW and IMPROVED www.MicroscopyEducation.com! And don't forget:  MME is now scheduling customized, on-site courses for the balance of the year.  Call me for a free assessment and quote.



At 08:14 PM 10/15/2009, you wrote:
Dear all,
Someone knows any way of visualization deposition or aggregates forms of copper disulfide or sulfide (CuS2 or CuS) by means of an optic microscope. In its natural form this compund has no autofluorescence. It colud be also any reaction that produce a color.

Thanks in advance
Best regards

--
Juan Luis Ribas
Servicio de Microscopía
Centro de Investigación, Tecnología e Innovación
Universidad de Sevilla
Av. Reina Mercedes 4b
41012 Sevilla

Tfno: 954559983